| dc.contributor.author | Akhbari, Kamran | |
| dc.contributor.author | Beheshti, Saeideh | |
| dc.contributor.author | Morsali, Ali | |
| dc.contributor.author | Yılmaz, Veysel T. | |
| dc.contributor.author | Büyükgüngör, Orhan | |
| dc.date.accessioned | 2020-06-21T13:53:05Z | |
| dc.date.available | 2020-06-21T13:53:05Z | |
| dc.date.issued | 2014 | |
| dc.identifier.issn | 0022-2860 | |
| dc.identifier.issn | 1872-8014 | |
| dc.identifier.uri | https://doi.org/10.1016/j.molstruc.2014.06.004 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12712/14959 | |
| dc.description | Yilmaz, Veysel/0000-0002-2849-3332 | en_US |
| dc.description | WOS: 000340315200035 | en_US |
| dc.description.abstract | A new lead(II) three-dimensional coordination polymer, [Pb-2(mu(3)-ANS)(2)(mu(2)-Cl)(2)(H2O)(2)](n) (1) [ANS(-) = 4-amino-1 -naphthalenesulfonateb has been synthesized and characterized. The single-crystal X-ray data of compound 1 shows only one type of Pb-II ion with coordination number of six, the lead atom has distorted octahedral coordination sphere containing stereo-chemically inactive electron lone pair. The thermal stability of 1 was studied by TG-DTA (Thermo gravimetric and differential thermal analyses). Regular morphology of Pb-2(SO4)O nano-particle was prepared from fine powders of compound 1 by calcination process at 700 degrees C. This nano-structure was characterized by XRD (X-ray powder diffraction) and SEM (Scanning electron microscopy). (C) 2014 Elsevier B.V. All rights reserved. | en_US |
| dc.description.sponsorship | University of TehranUniversity of Tehran [01/1/389845] | en_US |
| dc.description.sponsorship | The authors would like to acknowledge the financial support of University of Tehran for this research under grant number 01/1/389845 and supporting of this investigation by Tarbiat Modares University. | en_US |
| dc.language.iso | eng | en_US |
| dc.publisher | Elsevier | en_US |
| dc.relation.isversionof | 10.1016/j.molstruc.2014.06.004 | en_US |
| dc.rights | info:eu-repo/semantics/closedAccess | en_US |
| dc.subject | Lead(II) | en_US |
| dc.subject | Coordination polymer | en_US |
| dc.subject | Holodirected | en_US |
| dc.subject | Lead oxide sulfate | en_US |
| dc.subject | Nano-particle | en_US |
| dc.title | Holodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structures | en_US |
| dc.type | article | en_US |
| dc.contributor.department | OMÜ | en_US |
| dc.identifier.volume | 1074 | en_US |
| dc.identifier.startpage | 279 | en_US |
| dc.identifier.endpage | 283 | en_US |
| dc.relation.journal | Journal of Molecular Structure | en_US |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
