| dc.contributor.author | Sushkova, Svetlana N. | |
| dc.contributor.author | Vasilyeva, Galina K. | |
| dc.contributor.author | Minkina, Tatjana M. | |
| dc.contributor.author | Mandzhieva, Saglara S. | |
| dc.contributor.author | Tjurina, Irina G. | |
| dc.contributor.author | Kolesnikov, Sergei I. | |
| dc.contributor.author | Askin, Tayfun | |
| dc.date.accessioned | 2020-06-21T13:56:49Z | |
| dc.date.available | 2020-06-21T13:56:49Z | |
| dc.date.issued | 2014 | |
| dc.identifier.issn | 0375-6742 | |
| dc.identifier.issn | 1879-1689 | |
| dc.identifier.uri | https://doi.org/10.1016/j.gexplo.2014.02.018 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12712/15024 | |
| dc.description | Minkina, Tatiana/0000-0003-3022-0883; Mandzhieva, Saglara/0000-0001-6000-2209; Turina, Irina/0000-0003-4433-4849; Kolesnikov, Sergey/0000-0001-5860-8420; Sushkova, Svetlana/0000-0003-3470-9627; Turina, Irina/0000-0001-6884-8276; KIZILKAYA, RIDVAN/0000-0001-7475-9851; ASKIN, TAYFUN/0000-0001-9352-2710 | en_US |
| dc.description | WOS: 000339963600009 | en_US |
| dc.description.abstract | A new method for benzo[a] pyrene (BaP) analyses in plant material was developed using subcritical water extraction followed by HPLC analyses of the extracts. BaP extraction efficiency was determined by spiking grass vegetation collected from a preserve in Rostov Oblast (Russia). BaP recoverywas optimal with a 30-min extraction by water in a special steel cartridge at 250 degrees C and 100 atm. More than 98% of the BaP was recovered from the plant material using subcritical water extraction, compared to 72% recovery by saponification of the sample with conventional hexane extraction. Other advantages of subcritical water extraction are the use of water as an environmentally friendly solvent instead of large volumes of organic solvents as well as a shorter analysis time. (C) 2014 Elsevier B. V. All rights reserved. | en_US |
| dc.description.sponsorship | Ministry of Education and Science of RussiaMinistry of Education and Science, Russian Federation [1894]; Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [14-05-00586_a, 12-05-33078]; President of Russia [MK-6448.2014.4]; Leading Scientific School [2449.2014.4] | en_US |
| dc.description.sponsorship | We appreciate Prof. Pat Shea for the help in the manuscript preparation. This research was supported by projects of the Ministry of Education and Science of Russia, no. 1894, the Russian Foundation for Basic Research, no. 14-05-00586_a, and no. 12-05-33078, the President of Russia, no. MK-6448.2014.4 and the Leading Scientific School, no. 2449.2014.4. | en_US |
| dc.language.iso | eng | en_US |
| dc.publisher | Elsevier Science Bv | en_US |
| dc.relation.isversionof | 10.1016/j.gexplo.2014.02.018 | en_US |
| dc.rights | info:eu-repo/semantics/closedAccess | en_US |
| dc.subject | Benzo[a]pyrene | en_US |
| dc.subject | Plants | en_US |
| dc.subject | Subcritical water extraction | en_US |
| dc.subject | Hexane extraction | en_US |
| dc.title | New method for benzo[a] pyrene analysis in plant material using subcritical water extraction | en_US |
| dc.type | article | en_US |
| dc.contributor.department | OMÜ | en_US |
| dc.identifier.volume | 144 | en_US |
| dc.identifier.startpage | 267 | en_US |
| dc.identifier.endpage | 272 | en_US |
| dc.relation.journal | Journal of Geochemical Exploration | en_US |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
