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Aminophosphines Derived from N-Phenylpiperazine and N-Ethylpiperazine: Synthesis, Oxidation Reactions, and Molybdenum Complexes

Date

2011

Author

Sarioz, Ozlem
Oznergiz, Sena
Saracoglu, Hanife
Büyükgüngör, Orhan

Metadata

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Abstract

Functionalized aminophosphine of the type Ph2PNR2 (1,2) have been synthesized by treating Ph2PCl with N-phenylpiperazine or N-ethylpiperazine. Oxidation of these ligands with aqueous hydrogen peroxide, elemental sulfur or selenium afforded the corresponding phosphine oxides 3,4, sulfides 5,6, and selenides 7,8 in good yields. The molybdenum complexes of the aminophosphines have been obtained. All new compounds were fully characterized by IR, NMR, and microanalysis, and the molecular structures of two representative compounds were determined by single-crystal X-ray crystallography. (C) 2011 Wiley Periodicals, Inc. Heteroatom Chem 22: 679-686, 2011; View this article online at wileyonlinelibrary.com. DOI 10.1002/hc.20733

Source

Heteroatom Chemistry

Volume

22

Issue

6

URI

https://doi.org/10.1002/hc.20733
https://hdl.handle.net/20.500.12712/17405

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  • Scopus İndeksli Yayınlar Koleksiyonu [14046]
  • WoS İndeksli Yayınlar Koleksiyonu [12971]



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